Hydrochloric Acid → HCID 58128537, 화합물

HRID 1798805노트

반응식

HRID 1798805 반응식
C1(S[C:5]2[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][CH:6]=2)CC1.O[O:14][S:15]([O-:17])=O.[K+].Cl.C(O[CH2:24][CH3:25])(=O)C.[CH3:26]O>O>[CH:25]1([S:15]([C:5]2[CH:6]=[CH:7][C:8]([O:11][CH3:12])=[CH:9][CH:10]=2)(=[O:17])=[O:14])[CH2:24][CH2:26]1

참가 물질

7

반응물 5

HCID 313Hydrochloric AcidHCID 887MethanolHCID 8857Ethyl AcetateHCID 126929601-(Cyclopropylthio)-4-methoxybenzeneHCID 23707502Potassium hydroxy sulfite

생성물 1

HCID 58128537HCID 58128537, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

1-(cyclopropylthio)-4-methoxybenzene (300 mg, 1.66 mmol) was dissolved in 8 mL MeOH and Water (1:1). Oxone (4.9 g, 6.66 mmol) was added and the mixture was stirred overnight. 1N HCl was used to dissolve the salts and ethyl acetate was added to extract the product. The organic extract was washed with 1N HCl (3×) and brine, dried over sodium sulfate, and the solvent was removed under reduced pressure to obtain the crude product which is used without further purification.

후처리

  1. additionwas added
  2. extractionto extract the product
  3. extractionThe organic extract
  4. washwas washed with 1N HCl (3×) and brine
  5. dry with materialdried over sodium sulfate
  6. customthe solvent was removed under reduced pressure

출처 및 근거

ORD 기록
ord-db6dadd1b29d4c5ba5dd41448dc6262f
출처 데이터셋
uspto-grants-2013_01
특허 번호
US08343990B2

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