Hydrochloric Acid → HCID 68967848, 화합물

HRID 1804547노트

반응식

HRID 1804547 반응식
[O:1]=[C:2]1[N:6]([C:7]2[CH:8]=[C:9]([CH:19]=[CH:20][CH:21]=2)[CH2:10][NH:11]C(=O)OC(C)(C)C)[CH2:5][CH2:4][O:3]1.[ClH:22]>ClCCl>[ClH:22].[NH2:11][CH2:10][C:9]1[CH:8]=[C:7]([N:6]2[CH2:5][CH2:4][O:3][C:2]2=[O:1])[CH:21]=[CH:20][CH:19]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 57698624HCID 57698624, 화합물

생성물 1

HCID 68967848HCID 68967848, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

380 mg (1.30 mmol) tert-butyl [3-(2-oxo-oxazolidin-3-yl)-benzyl]-carbamate are placed in 2 ml dichloromethane, 4.00 ml (8 mmol) 2 molar ethereal hydrochloric acid are added. The mixture is stirred for 16 hours at ambient temperature, then evaporated down. The residue is lyophilised.

후처리

  1. customevaporated down

출처 및 근거

ORD 기록
ord-6f3fc64086294ee1a9b589c317efbcce
출처 데이터셋
uspto-grants-2013_01
특허 번호
US08354418B2

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