Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-([[3-Chloro-4-(trifluoromethyl)benzyl]amino]carbonyl)benzenesulfonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Chloro-4-(trifluoromethyl)benzylamine | HCID 23512744 | — |
| 반응물 | Potassium 4-carboxybenzenesulfonate | HCID 23670833 | — |
| 생성물 | 4-([[3-Chloro-4-(trifluoromethyl)benzyl]amino]carbonyl)benzenesulfonyl chloride | HCID 57731928 | 45% |
반응 단계
The title compound was prepared from 4-sulphobenzoic acid monopotassium salt and 3-chloro-4-(trifluoromethyl)benzylamine in 45% yield following the procedure described in Preparation 1. The thionyl chloride solution was heated at reflux for 3 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08357711B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-844ee162ab384fb5a4d3f504c3d6312c |
| 출처 메모 | uspto-grants-2013_01 |