Ammonium Acetate → 9-Aminospiro[4.5]dec-8-EN-7-one

HRID 1817807

반응식

HRID 1817807 반응식
CN(C)[C:3]1[CH:8]=[CH:7][C:6]([CH:9]2[CH2:14][C:13](=[O:15])[CH2:12][C:11](=O)[CH2:10]2)=CC=1.C1C2(CC(=O)CC(=O)C2)CCC1.C([O-])(=O)C.[NH4+:34]>>[NH2:34][C:11]1[CH2:10][C:9]2([CH2:6][CH2:7][CH2:8][CH2:3]2)[CH2:14][C:13](=[O:15])[CH:12]=1

참가 물질

4

반응물 3

HCID 517165Ammonium AcetateHCID 7301175-(4-(Dimethylamino)phenyl)-1,3-cyclohexanedioneHCID 4831594Spiro[4.5]decane-7,9-dione

생성물 1

HCID 578832909-Aminospiro[4.5]dec-8-EN-7-one

실험 절차

In analogy to (Baraldi, P. G.; Simoni, D.; Manfredini, S.; Synthesis 1983, (11) 902-903 spiro[4.5]decane-7,9-dione was reacted with ammonium acetate to give the title compound as a colorless solid.

출처 및 근거

ORD 기록
ord-6175484f394d4eb691a663225203d72e
출처 데이터셋
uspto-grants-2009_10
특허 번호
US07598384B2

연결된 노트

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