Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2,5-Dimethyl-4-(2-morpholin-4-yl-ethoxy)aniline dihydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | N-{2,5-Dimethyl-4-[2-(morpholin-4-yl)ethoxy]phenyl}acetamide | HCID 22169683 | — |
| 생성물 | 2,5-Dimethyl-4-(2-morpholin-4-yl-ethoxy)aniline dihydrochloride | HCID 22169674 | — |
반응 단계
The mixture of N-[2,5-dimethyl-4-(2-morpholin-4-yl-ethoxy)-phenyl]-acetamide (11.4 g, 39 mmol) in 3N aq.HCl (100 mL) was refluxed for 2 h and then concentrated under reduced pressure. The residue was lyophilized to give 2,5-dimethyl-4-(2-morpholin-4-yl-ethoxy)aniline dihydrochloride as gray solid quantitatively.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07037909B2 |
| 출처 데이터셋 | uspto-grants-2006_05 |
| ORD ID | ord-81c71f63cc804866bd3cc3fc12965995 |
| 출처 메모 | uspto-grants-2006_05 |