Methyl iodide → HCID 22142153, 화합물

반응식

[F:1][C:2]([F:25])([F:24])[C:3]1[CH:4]=[C:5]([CH:21]=[CH:22][CH:23]=1)[O:6][C:7]1[CH:12]=[CH:11][C:10]([NH:13][NH:14][C:15]([O:17][CH:18]([CH3:20])[CH3:19])=[O:16])=[CH:9][CH:8]=1.[CH3:26]I>>[CH3:26][N:13]([C:10]1[CH:11]=[CH:12][C:7]([O:6][C:5]2[CH:21]=[CH:22][CH:23]=[C:3]([C:2]([F:24])([F:25])[F:1])[CH:4]=2)=[CH:8][CH:9]=1)[NH:14][C:15]([O:17][CH:18]([CH3:20])[CH3:19])=[O:16]

참가 물질

반응물 2

HCID 6328Methyl iodide

HCID 22142146HCID 22142146, 화합물

생성물 1

HCID 22142153HCID 22142153, 화합물

실험 절차

The product (0.4 g) of Step 4 of Example 1 was heated in methyl iodide (5 mL) at reflux for 1 day and then concentrated under reduced pressure to give a red oil (0.5 g).

후처리

temperatureat reflux for 1 day
concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록: ord-6d49388296914a1ba606a24263907cbc
출처 데이터셋: uspto-grants-2006_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07045512B2

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