4-Nitro-3-trifluoromethylphenol → 4-(3-Fluoro-benzyloxy)-1-nitro-2-trifluoromethyl-benzene

HRID 1827391

반응식

HRID 1827391 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][C:5]=1[C:11]([F:14])([F:13])[F:12])([O-:3])=[O:2].[F:15][C:16]1[CH:17]=[C:18]([CH:21]=[CH:22][CH:23]=1)[CH2:19]Br>>[F:15][C:16]1[CH:17]=[C:18]([CH:21]=[CH:22][CH:23]=1)[CH2:19][O:10][C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[C:5]([C:11]([F:12])([F:13])[F:14])[CH:6]=1

참가 물질

3

반응물 2

HCID 69314-Nitro-3-trifluoromethylphenolHCID 680073-Fluorobenzyl bromide

생성물 1

HCID 221379634-(3-Fluoro-benzyloxy)-1-nitro-2-trifluoromethyl-benzene수율 85%

실험 절차

Prepared in analogy to example 8 from 4-nitro-3-(trifluoromethyl)-phenol and 3-Fluoro-benzylbromide. Yield=85%. Yellowish solid. MS (ISP): m/e=333.2 (M++NH4).

출처 및 근거

ORD 기록
ord-36c9b3c82f3f4eb4be7c7471c86524dc
출처 데이터셋
uspto-grants-2006_05
특허 번호
US07053245B2

연결된 노트

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