Methacrylic Acid → 1-Butoxyethyl methacrylate

반응식

[CH2:1]([O:5][CH:6]=[CH2:7])[CH2:2][CH2:3][CH3:4].[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]>>[C:8]([O:13][CH:6]([O:5][CH2:1][CH2:2][CH2:3][CH3:4])[CH3:7])(=[O:12])[C:9]([CH3:11])=[CH2:10]

참가 물질

반응물 2

HCID 4093Methacrylic Acid

HCID 8108Butyl vinyl ether

생성물 1

HCID 219599501-Butoxyethyl methacrylate

실험 절차

The reaction procedure of Example 1 was repeated using equimolar amounts of n-butylvinyl ether and methacrylic acid. The structure of the product, 1-n-butoxyethyl methacrylate (Compound C) was obtained in 88% yield. Compound C is an example of a mono-functional alpha-alkoxyalkyl(meth)acrylate which may optionally be included with multi-functional alpha-alkoxyalkyl(meth)acrylate compounds in compositions of the present invention. The structure of Compound C was confirmed by 1H NMR and infrared analysis.

후처리

customThe reaction procedure of Example 1

출처 및 근거

ORD 기록: ord-290fa3e56ef54cc2ab37f996c368b87c
출처 데이터셋: uspto-grants-2006_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07067601B2

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