Potassium Bromide → HCID 57455831, 화합물

HRID 1831262

반응식

HRID 1831262 반응식
Cl[C:2]([O:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][N:13]=2)=[CH:7][CH:6]=1)=[O:3].[Cl:22][C:23]1[CH:35]=[CH:34][CH:33]=[C:32]([F:36])[C:24]=1[CH2:25][N:26]1[CH2:31][CH2:30][NH:29][CH2:28][CH2:27]1.[K+].[Br-]>C(O)C>[F:19][C:18]([F:21])([F:20])[C:15]1[CH:16]=[CH:17][C:12]([O:11][C:8]2[CH:9]=[CH:10][C:5]([O:4][C:2]([N:29]3[CH2:28][CH2:27][N:26]([CH2:25][C:24]4[C:32]([F:36])=[CH:33][CH:34]=[CH:35][C:23]=4[Cl:22])[CH2:31][CH2:30]3)=[O:3])=[CH:6][CH:7]=2)=[N:13][CH:14]=1

참가 물질

5

반응물 3

HCID 253877Potassium BromideHCID 7357371-((2-Chloro-6-fluorophenyl)methyl)piperazineHCID 220477624-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformate

생성물 1

HCID 57455831HCID 57455831, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The hydrochloride of the title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-(2-chloro-6-fluorobenzyl)piperazine. White crystals, m.p. 204–205° C. (from ethanol); HPLC-MS m/z=510 (M+H); IR (KBr): ν 1726 (C═O) cm−1;

출처 및 근거

ORD 기록
ord-7168c1c05d8e4081ba020e1c3875c208
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07067517B2

연결된 노트

불러오는 중…