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Dimethylformamide → 4-(2,3,4-Trimethoxy-6-methylbenzoyl)-2,3-dichloro-5-methoxypyridine

HRID 1835427
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인쇄 미리보기

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HRID 1835427 반응식
CN(C)C=O.P(Cl)(Cl)([Cl:8])=O.[CH3:11][O:12][C:13]1[C:30]([O:31][CH3:32])=[C:29]([O:33][CH3:34])[CH:28]=[C:27]([CH3:35])[C:14]=1[C:15]([C:17]1[C:22]([O:23][CH3:24])=[CH:21][N+:20]([O-])=[CH:19][C:18]=1[Cl:26])=[O:16]>C1(C)C=CC=CC=1>[CH3:11][O:12][C:13]1[C:30]([O:31][CH3:32])=[C:29]([O:33][CH3:34])[CH:28]=[C:27]([CH3:35])[C:14]=1[C:15]([C:17]1[C:22]([O:23][CH3:24])=[CH:21][N:20]=[C:19]([Cl:8])[C:18]=1[Cl:26])=[O:16]
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참가 물질

5

반응물 3

HCID 6228DimethylformamideHCID 24813Phosphorus oxychlorideHCID 235035884-(2,3,4-trimethoxy-6-methylbenzoyl)-3-chloro-5-methoxypyridine-N-oxide

생성물 1

HCID 235035954-(2,3,4-Trimethoxy-6-methylbenzoyl)-2,3-dichloro-5-methoxypyridine수율 739.8%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

5 ml of dimethylformamide was added to 2.5 ml of toluene, the mixture was cooled with ice, and 1.3 ml (1.4 mmol) of phosphorus oxychloride was dropwise added thereto. After the mixture was stirred under cooling with ice for 10 minutes, 2.5 g (0.7 mmol) of 4-(2,3,4-trimethoxy-6-methylbenzoyl)-3-chloro-5-methoxypyridine-N-oxide was added thereto. After the mixture was stirred under cooling with ice for 30 minutes, the temperature was recovered to room temperature, followed by stirring for 2 hours. 30 ml of water was added to the mixture to terminate the reaction, and ethyl acetate was added thereto for extraction. The organic layer was dried over anhydrous sodium sulfate, subjected to filtration and purified by silica gel column chromatography to obtain 2.0 g (yield 76%) of 4-(2,3,4-trimethoxy-6-methylbenzoyl)-2,3-dichloro-5-methoxypyridine (compound No. 193; m.p. 98-99° C.).

후처리

  1. additionwas dropwise added
  2. temperatureunder cooling with ice for 10 minutes
  3. stirringAfter the mixture was stirred
  4. temperatureunder cooling with ice for 30 minutes
  5. customthe temperature was recovered to room temperature
  6. stirringby stirring for 2 hours
  7. addition30 ml of water was added to the mixture
  8. customto terminate
  9. customthe reaction, and ethyl acetate
  10. additionwas added
  11. extractionfor extraction
  12. dry with materialThe organic layer was dried over anhydrous sodium sulfate
  13. filtrationsubjected to filtration
  14. custompurified by silica gel column chromatography

출처 및 근거

ORD 기록
ord-4e29c744629d4a6ba339a90cd7aeb21d
출처 데이터셋
uspto-grants-2004_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06770662B2

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