Hydrochloric Acid → HCID 178507240, 화합물

HRID 1837507노트

반응식

HRID 1837507 반응식
Cl.[N+:2]([C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[CH2:10][CH:9]([C:14]1[N:15]=[CH:16][NH:17][CH:18]=1)[CH2:8]2)([O-])=O>C(O)C.[Pd]>[NH:17]1[CH:18]=[C:14]([CH:9]2[CH2:8][C:7]3[C:11](=[CH:12][CH:13]=[C:5]([NH2:2])[CH:6]=3)[CH2:10]2)[N:15]=[CH:16]1

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 178526436HCID 178526436, 화합물

생성물 1

HCID 178507240HCID 178507240, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

The hydrochloride of the product obtained in Step 3 is stirred under a hydrogen atmosphere in the presence of 10% palladium-on-carbon in ethanol. After filtration and concentration of the solvent, the product is used as it is in the following Step.

후처리

  1. filtrationAfter filtration and concentration of the solvent

출처 및 근거

ORD 기록
ord-242418fba3d34fc9b4850ed85f169832
출처 데이터셋
uspto-grants-2004_08
특허 번호
US06784183B2

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