Hydrochloric Acid → HCID 178526618, 화합물
반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]2[N:13]=[CH:14][N:15](C(C3C=CC=CC=3)(C3C=CC=CC=3)C3C=CC=CC=3)[CH:16]=2)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].Cl>CO>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]2[N:13]=[CH:14][NH:15][CH:16]=2)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]참가 물질
4
실험 절차
A mixture of 11 g of the product obtained in Step 3, 6 ml of concentrated hydrochloric acid and 150 ml of methanol is heated at reflux for 2 hours. The solvent is concentrated and the residue is taken up in an isopropanol/diethyl ether mixture. The expected product is obtained by filtering off the precipitate that has formed.
후처리
- temperatureis heated
- temperatureat reflux for 2 hours
- concentrationThe solvent is concentrated
출처 및 근거
- ORD 기록
- ord-0af9401dae884228ac9b80e269f20f5d
- 출처 데이터셋
- uspto-grants-2004_08
- 특허 번호
- US06784183B2
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