Nitromethane → HCID 66692011, 화합물

HRID 1843937노트

반응식

HRID 1843937 반응식
[F:1][C:2]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[CH:6][C:3]=1[CH:4]=O.[N+:12]([CH3:15])([O-:14])=[O:13].[OH-].[Na+]>>[F:1][C:2]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[CH:6][C:3]=1[CH:4]=[CH:15][N+:12]([O-:14])=[O:13]

참가 물질

4

반응물 3

HCID 6375NitromethaneHCID 14798Sodium HydroxideHCID 27348722-Fluoro-5-methoxybenzaldehyde

생성물 1

HCID 66692011HCID 66692011, 화합물수율 58.7%

실험 절차

2-Fluoro-5-methoxy-benzaldehyde (4 g, 25.95 mmol) was reacted with nitro methane (1.58 g, 25.95 mmol), 10N NaOH (2.2 mL, 27.24 mmol) to afford 3 g of the product (58.7% yield).

출처 및 근거

ORD 기록
ord-95563d6c339a463f9e109f1393174b1a
출처 데이터셋
uspto-grants-2015_02
특허 번호
US08946260B2

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