Methyl iodide → 4-Bromo-2-iodo-1-methoxybenzene
반응식
IC.[Br:3][C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[C:6]([I:11])[CH:5]=1.[C:12](=O)([O-])[O-].[K+].[K+]>CC(C)=O>[Br:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][CH3:12])=[C:6]([I:11])[CH:5]=1참가 물질
5
실험 절차
Iodomethane (103 μL, 1.65 mmol) was added to a solution of 4-bromo-2-iodophenol (450 mg, 1.51 mmol) and potassium carbonate (271 mg, 1.96 mmol) in acetone (10 mL). The resulting mixture was stirred at room temperature for 16 hours.
출처 및 근거
- ORD 기록
- ord-f0f078d4c50d404293eb3ff18ce964e5
- 출처 데이터셋
- uspto-grants-2015_02
- 특허 번호
- US08952008B2
반응 노트
불러오는 중…