HCID 13066945, 화합물 → 2-Methyl-3-hydroxy-4-formyl-5-vinylpyridine
반응식
[CH3:1][C:2]1[C:7]([OH:8])=[C:6]([CH2:9][OH:10])[C:5]([CH:11]=[CH2:12])=[CH:4][N:3]=1>[O-2].[O-2].[Mn+4].C(Cl)(Cl)Cl>[CH3:1][C:2]1[C:7]([OH:8])=[C:6]([CH:9]=[O:10])[C:5]([CH:11]=[CH2:12])=[CH:4][N:3]=1참가 물질
4
실험 절차
A solution of 10 g. of 2-methyl-3-hydroxy-4-hydroxymethyl-5-vinylpyridine in 300 ml. of hot chloroform was treated with 100 g. of manganese dioxide. After 1/2 hour of stirring, the mixture was filtered and the filtrate was evaporated to dryness to give 2-methyl-3-hydroxy-4-formyl-5-vinylpyridine.
후처리
- filtrationthe mixture was filtered
- customthe filtrate was evaporated to dryness
출처 및 근거
- ORD 기록
- ord-e62f1e16e6414823b734459651b3d223
- 출처 데이터셋
- uspto-grants-1980_08
- 특허 번호
- US04217352
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