Diisopropylamine → HCID 23346036, 화합물

HRID 1856140

반응식

HRID 1856140 반응식
[C:1]1([N:10]=[C:11]=[S:12])[CH:6]=[CH:5][C:4]([N:7]=[C:8]=[S:9])=[CH:3][CH:2]=1.[CH:13]([NH:16][CH:17]([CH3:19])[CH3:18])([CH3:15])[CH3:14]>C(#N)C>[C:4]1([NH:7][C:8]([N:16]([CH:17]([CH3:19])[CH3:18])[CH:13]([CH3:15])[CH3:14])=[S:9])[CH:3]=[CH:2][C:1]([NH:10][C:11]([N:16]([CH:17]([CH3:19])[CH3:18])[CH:13]([CH3:15])[CH3:14])=[S:12])=[CH:6][CH:5]=1

참가 물질

4

반응물 2

HCID 7912DiisopropylamineHCID 19958p-Phenylene diisothiocyanate

생성물 1

HCID 23346036HCID 23346036, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

To a solution of 1.92 g. of 1,4-phenylenediisothiocyanate in 100 ml. of acetonitrile is added 2.5 g. of diisopropylamine. On standing, a precipitate forms which is filtered off and crystallized from acetone-cyclohexane to yield 2.7 g. of the title compound, melting point 185° C.

후처리

  1. filtrationa precipitate forms which is filtered off
  2. customcrystallized from acetone-cyclohexane
  3. customto yield 2.7 g

출처 및 근거

ORD 기록
ord-eb2cf8b6e22245c39b51d070cdc91d54
출처 데이터셋
uspto-grants-1980_08
특허 번호
US04218396

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