Hydrochloric Acid → HCID 23500354, 화합물
반응식
[C:1]1([CH:9]=[C:7]([OH:8])[CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].O=[C:11]1[CH2:16][CH2:15][CH:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH:12]1[C:23](OCC)=[O:24].Cl>C(O)C>[OH:2][C:1]1[C:9]2[C:11]3[CH2:16][CH2:15][CH:14]([C:17]4[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH2:13][C:12]=3[C:23](=[O:24])[O:8][C:7]=2[CH:6]=[C:4]([OH:5])[CH:3]=1참가 물질
5
실험 절차
A solution of phloroglucinol (1.56 g) and ethyl 2-oxo-5-phenylcyclo-hexane-carboxylate (2.52 g) in ethanol (25 ml) was treated with dry HCl as described in example 1a. The precipitate was filtered and washed with water and EtOH. Yield 1.0 g (32%).
후처리
- filtrationThe precipitate was filtered
- washwashed with water and EtOH
출처 및 근거
- ORD 기록
- ord-c4f62ee5ff3246d1beeb118065637b4e
- 출처 데이터셋
- uspto-grants-2003_03
- 특허 번호
- US06538022B1
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