4-Morpholinecarbonyl chloride → HCID 69664348, 화합물

반응식

[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:19])=[C:6]([CH:18]=1)[C:7]([NH:9][C:10]1[CH:15]=[C:14]([Cl:16])[CH:13]=[C:12]([Cl:17])[CH:11]=1)=[O:8].[N:20]1([C:26](Cl)=[O:27])[CH2:25][CH2:24][O:23][CH2:22][CH2:21]1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:19][C:26]([N:20]2[CH2:25][CH2:24][O:23][CH2:22][CH2:21]2)=[O:27])=[C:6]([CH:18]=1)[C:7]([NH:9][C:10]1[CH:15]=[C:14]([Cl:16])[CH:13]=[C:12]([Cl:17])[CH:11]=1)=[O:8]

참가 물질

반응물 2

HCID 848104-Morpholinecarbonyl chloride

HCID 28046665-chloro-N-(3,5-dichlorophenyl)-2-hydroxybenzamide

생성물 1

HCID 69664348HCID 69664348, 화합물수율 83.2%

실험 절차

Using 5-chloro-N-(3,5-dichlorophenyl)-2-hydroxybenzamide and morpholine-4-carbonyl chloride as the raw materials, the same operation as the Example 71 gave the title compound.

출처 및 근거

ORD 기록: ord-240ef8f4420340a9a7ec3aa74f270784
출처 데이터셋: uspto-grants-2009_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07626042B2

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