Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl behenate → (2-Morpholinoethyl) behenate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl behenate | HCID 13584 | — |
| 반응물 | 2-Morpholinoethanol | HCID 61163 | — |
| 촉매 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | (2-Morpholinoethyl) behenate | HCID 66705417 | 91% |
반응 단계
A mixture of 35.5 g of methyl behenate (18), 19.7 g of 2-morpholinoethanol (17), 270 mg of sodium methoxide and 150 g of toluene was heated under reflux for 6 hours while distilling off the methanol resulting from the reaction. The reaction solution was cooled. By standard aqueous work-up and distilling off toluene, 41.3 g of (2-morpholinoethyl) behenate (Quencher 2) was obtained (yield 91%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07629108B2 |
| 출처 데이터셋 | uspto-grants-2009_12 |
| ORD ID | ord-a386f213e6bd46459c2ea17f0bb9ba1b |
| 출처 메모 | uspto-grants-2009_12 |