Benzoyl chloride → 4-(6-(Benzoyloxy)benzo[b]thiophen-2-yl)phenyl benzoate

반응식

[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[S:12][C:11]3[CH:13]=[C:14]([OH:17])[CH:15]=[CH:16][C:10]=3[CH:9]=2)=[CH:4][CH:3]=1.[C:18](Cl)(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:18]([O:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[S:12][C:11]3[CH:13]=[C:14]([O:17][C:18](=[O:25])[C:19]4[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=4)[CH:15]=[CH:16][C:10]=3[CH:9]=2)=[CH:4][CH:3]=1)(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

참가 물질

반응물 2

HCID 7412Benzoyl chloride

HCID 4459202-(4-Hydroxyphenyl)benzo(b)thiophen-6-ol

생성물 1

HCID 99116044-(6-(Benzoyloxy)benzo[b]thiophen-2-yl)phenyl benzoate

실험 절차

2-(4-Hydroxyphenyl)-6-hydroxybenzo[b]thiophene and benzoyl chloride were converted to the title compound by the procedure of Example 3 to yield a white crystalline solid. mp 216° C.-218° C.

출처 및 근거

ORD 기록: ord-acc539a2d2ac4cc98f488697cecbd01f
출처 데이터셋: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06096781

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