Sodium hydride → HCID 18694775, 화합물

HRID 1871029노트

반응식

HRID 1871029 반응식
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:4][CH:3]=1.[H-].[Na+].Br[CH2:16][CH2:17][CH2:18][CH2:19][NH:20]C(=O)C1C(=CC=CC=1)C(N)=O>>[F:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[N:9]=[CH:10][N:11]([CH2:16][CH2:17][CH2:18][CH2:19][NH2:20])[CH:12]=2)=[CH:6][CH:7]=1

참가 물질

4

반응물 3

HCID 24758Sodium hydrideHCID 18694800HCID 18694800, 화합물HCID 178418867HCID 178418867, 화합물

생성물 1

HCID 18694775HCID 18694775, 화합물수율 81.8%

실험 절차

Using the procedure of Stage A of Example 1, 10 g of the product of Stage A, 1.95 g of sodium hydride and 11.80 g of N-4-bromobutyl-phthalamide were reacted to obtain 7.53 g of the expected product melting at 138-140° C.

후처리

  1. customwere reacted

출처 및 근거

ORD 기록
ord-a246439f7daf433b97081e55f574c02a
출처 데이터셋
uspto-grants-2000_08
특허 번호
US06100404

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