Isobutyraldehyde → 1,1-Dimethylethyl 2-(2-methylpropylidene)hydrazinecarboxylate

HRID 1874084노트

반응식

HRID 1874084 반응식
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[C:6]([O:10][C:11](=[O:14])[NH:12][NH2:13])([CH3:9])([CH3:8])[CH3:7]>>[C:6]([O:10][C:11]([NH:12][N:13]=[CH:1][CH:2]([CH3:4])[CH3:3])=[O:14])([CH3:9])([CH3:8])[CH3:7]

참가 물질

3

반응물 2

HCID 6561IsobutyraldehydeHCID 70091tert-Butyl carbazate

생성물 1

HCID 852555401,1-Dimethylethyl 2-(2-methylpropylidene)hydrazinecarboxylate

실험 절차

B-21a is prepared analogously to B-19a starting from isobutyraldehyde (1.26 mL, 13.9 mmol) and tert-butylcarbazate (1.83 g, 13.9 mmol). Yield: 2.56 g.

후처리

  1. customB-21a is prepared analogously to B-19a

출처 및 근거

ORD 기록
ord-ba3fd5808a4c483da23791ef3b674f87
출처 데이터셋
uspto-grants-2012_11
특허 번호
US08304556B2

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