반응식
[CH3:1][N:2]1[C:6]([C:7]([NH:9][C:10]2[CH:15]=[C:14]([O:16][C:17]3[CH:18]=[N:19][C:20]([N+:23]([O-])=O)=[CH:21][CH:22]=3)[CH:13]=[C:12]([CH3:26])[CH:11]=2)=[O:8])=[CH:5][C:4]([CH3:27])=[N:3]1>[C].[Pd].CO>[NH2:23][C:20]1[N:19]=[CH:18][C:17]([O:16][C:14]2[CH:15]=[C:10]([NH:9][C:7]([C:6]3[N:2]([CH3:1])[N:3]=[C:4]([CH3:27])[CH:5]=3)=[O:8])[CH:11]=[C:12]([CH3:26])[CH:13]=2)=[CH:22][CH:21]=1참가 물질
4
실험 절차
In the same manner as in Reference Example 13 and using 1,3-dimethyl-N-{3-methyl-5-[(6-nitropyridin-3-yl)oxy]phenyl}-1H-pyrazole-5-carboxamide (7.63 g, 17.3 mmol), palladium carbon (50% water-containing product, 1.88 g) and methanol (50 mL) as starting materials, the title compound (6.25 g, 88%) was obtained as a pale-yellow oil.
출처 및 근거
- ORD 기록
- ord-6e07c7d512194af3a7374910ab217d12
- 출처 데이터셋
- uspto-grants-2012_11
- 특허 번호
- US08304557B2
연결된 노트
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