Methyl iodide → HCID 68590834, 화합물
반응식
[CH3:1][C:2]1[C:7]2[S:8][CH:9]=[CH:10][C:6]=2[CH2:5][CH2:4][N:3]=1.[CH3:11][I:12]>C(OCC)(=O)C>[I-:12].[CH3:11][N+:3]1[CH2:4][CH2:5][C:6]2[CH:10]=[CH:9][S:8][C:7]=2[C:2]=1[CH3:1]참가 물질
4
실험 절차
A mixture of 4.64 g (31 mmol) 7-methyl-4,5-dihydro-thieno[2,3-c]pyridine (prepared analogously to J.Am.Chem.Soc., 1951, 1257), 8.0 ml (128 mmol) methyl iodide and 20 ml of ethyl acetate is stirred for 15 min. The precipitate formed is suction filtered, washed with ethyl acetate and dried in vacuo.
후처리
- customprepared analogously to J.Am.Chem.Soc
- customThe precipitate formed
- filtrationfiltered
- washwashed with ethyl acetate
- customdried in vacuo
출처 및 근거
- ORD 기록
- ord-0843bf2fcfc94ff0ada02d33864cdc05
- 출처 데이터셋
- uspto-grants-2012_11
- 특허 번호
- US08309542B2
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