Methyl iodide → 5,6-Dimethyl-4,5-dihydro-thieno[2,3-c]pyridinium iodide
반응식
[CH3:1][CH:2]1[N:7]=[CH:6][C:5]2[S:8][CH:9]=[CH:10][C:4]=2[CH2:3]1.[CH3:11][I:12]>C(#N)C>[I-:12].[CH3:1][CH:2]1[N+:7]([CH3:11])=[CH:6][C:5]2[S:8][CH:9]=[CH:10][C:4]=2[CH2:3]1참가 물질
4
실험 절차
A solution of 4.0 g (26.5 mmol) 5-methyl-4,5-dihydro-thieno[2,3-c]-pyridine in 250 ml acetonitrile is combined at RT with 16.5 ml (264.5 mmol) methyl iodide and stirred for 30 min. The precipitate formed is filtered off and washed with acetonitrile.
후처리
- customThe precipitate formed
- filtrationis filtered off
- washwashed with acetonitrile
출처 및 근거
- ORD 기록
- ord-9e8eb94d090b4b9ebc5e1659be9e08e3
- 출처 데이터셋
- uspto-grants-2012_11
- 특허 번호
- US08309542B2
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