Hydrochloric Acid → HCID 69203826, 화합물

HRID 1875553노트

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HRID 1875553 반응식
[CH3:1][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([O:10]C)=[O:9])[CH3:3].[ClH:18]>>[ClH:18].[CH3:3][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([OH:10])=[O:9])[CH3:1]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 23144875HCID 23144875, 화합물

생성물 1

HCID 69203826HCID 69203826, 화합물

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온도
100 °C

실험 절차

The mixture of methyl 3-dimethylaminomethyl-2-nitrobenzoate (0.72 g) and 6M hydrochloric acid was stirred at 100° C. overnight. After cooling the mixture to room temperature, the precipitated crystals were filtered out, washed with diethylether and dried under reduced pressure to obtain 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride.

후처리

  1. temperatureAfter cooling the mixture to room temperature
  2. filtrationthe precipitated crystals were filtered out
  3. washwashed with diethylether
  4. customdried under reduced pressure

출처 및 근거

ORD 기록
ord-bd892fdec45446f8a5fee6d5f6191d21
출처 데이터셋
uspto-grants-2012_11
특허 번호
US08309561B2

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