N-vinyl-2-pyrrolidone → 1,3,5-Trimethoxybenzene

HRID 1882644노트

반응식

HRID 1882644 반응식
C=CN1CCCC1=O.O=S(=O)(Oc1ccccc1)C(F)(F)F>CC(C)(C)P1CN(c2ccc(C(F)(F)F)cc2)CP(C(C)(C)C)CN(c2ccc(C(F)(F)F)cc2)C1.CCN(CC)CC.Cc1ccccc1.C1=C\CC/C=C\CC/1.C1=C\CC/C=C\CC/1.[Ni]>COc1cc(OC)cc(OC)c1.O=C1CCCN1/C=C/c1ccccc1.C=C(c1ccccc1)N1CCCC1=O

참가 물질

9

반응물 2

HCID 6917N-vinyl-2-pyrrolidoneHCID 548641Phenyl Trifluoromethanesulfonate

생성물 3

HCID 693011,3,5-TrimethoxybenzeneHCID 5371898HCID 5371898, 화합물HCID 110196022-Pyrrolidinone, 1-(1-phenylethenyl)-

시약·촉매·용매 4

HCID 8471Triethylamine시약HCID 1778483303,7-Di-tert-butyl-1,5-bis(4-(trifluoromethyl)phenyl)-1,5,3,7-diazadiphosphocane촉매HCID 1140Toluene용매HCID 6433264Bis(1,5-cyclooctadiene)nickel기타

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온도
85 °C

후처리

  1. additionFiltrate 상 유지

출처 및 근거

ORD 기록
ord-c586ea418fc84e1083ce5d8afe7196e8
출처 데이터셋
N-vinyl pyrrolidone Mizoroki-Heck

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