Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Fluoronitrobenzene → 1-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Fluoronitrobenzene | HCID 9590 | — |
| 반응물 | 4-(Trifluoromethyl)benzenemethanol | HCID 67684 | — |
| 반응물 | 1-(3-Fluorobenzyloxy)-4-nitro-benzene | HCID 22137915 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzene | HCID 2743792 | — |
반응 단계
Prepared in analogy to 1-(3-fluorobenzyloxy)-4-nitro-benzene, starting from 4-fluoro nitrobenzene and 4-trifluoromethyl benzyl alcohol. Yield after recristallisation from methanol: 82% of a brownish solid. Mp=80.5-81.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06762320B2 |
| 출처 데이터셋 | uspto-grants-2004_07 |
| ORD ID | ord-81efb0f73cfe484fbf072873c52f0f78 |
| 출처 메모 | uspto-grants-2004_07 |