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HRID1884103

反应详情

EQUATION

反应方程式

HRID 1884103 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(F)cc1
HCID9590

1-Fluoro-4-nitrobenzene

C6H4FNO2

结构：OCc1ccc(C(F)(F)F)cc1
HCID67684

4-(Trifluoromethyl)benzyl alcohol

C8H7F3O

结构：O=[N+]([O-])c1ccc(OCc2cccc(F)c2)cc1
HCID22137915

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(OCc2ccc(C(F)(F)F)cc2)cc1
HCID2743792

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Prepared in analogy to 1-(3-fluorobenzyloxy)-4-nitro-benzene, starting from 4-fluoro nitrobenzene and 4-trifluoromethyl benzyl alcohol. Yield after recristallisation from methanol: 82% of a brownish solid. Mp=80.5-81.5° C.