2-Acetamido-6-chlorobenzoic acid → HCID 53444447, 화합물
반응식
[Cl:1][C:2]1[C:7]([C:8]([OH:10])=[O:9])=[C:6]([NH:11]C(C)=O)[CH:5]=[CH:4][CH:3]=1>Cl>[ClH:1].[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]([NH2:11])[C:7]=1[C:8]([OH:10])=[O:9]참가 물질
3
실험 절차
A mixture of 20.0 grams (0.093 mole) of 6-chloro-2-(methylcarbonylamino)benzoic acid in 150 mL of concentrated hydrochloric acid was stirred at 80° for about 3 hours. The reaction mixture was cooled to ambient temperature and was filtered to collect a solid. The solid was washed with cold diethyl ether and dried to yield 20.3 grams of 6-chloroanthranilic acid hydrochloride; m.p. 194°-195° C. The nmr spectrum was consistent with the proposed structure.
후처리
- filtrationwas filtered
- customto collect a solid
- washThe solid was washed with cold diethyl ether
- customdried
출처 및 근거
- ORD 기록
- ord-e801423cdd2448cebe8ec3c4e2b27195
- 출처 데이터셋
- uspto-grants-1992_09
- 특허 번호
- US05149357
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