Acetic Anhydride → 7-Methoxy-2-acetamido-tetralin

HRID 1886483

반응식

[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][CH:9]([NH2:13])[CH2:10]2)=[CH:5][CH:4]=1.[C:14](OC(=O)C)(=[O:16])[CH3:15]>>[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][CH:9]([NH:13][C:14](=[O:16])[CH3:15])[CH2:10]2)=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 7918Acetic Anhydride

HCID 116080152-Amino-7-methoxytetralin

생성물 1

HCID 100136977-Methoxy-2-acetamido-tetralin수율 51%

실험 절차

Using a procedure similar to that described in Example 1, 0.40 g of 7-methoxy-2-amino-tetralin yielded 0.21 g (51%) of 7-methoxy-2-acetamido-tetralin following treatment with acetic anhydride.

출처 및 근거

ORD 기록: ord-436b62d67dcb4511afe855af84c94d34
출처 데이터셋: uspto-grants-1992_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05151446

연결된 노트

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