N-methyl-2-pyrrolidone → NMP Methanol

HRID 1886768

반응식

HRID 1886768 반응식
[CH3:1][N:2]1[C:6](=[O:7])[CH2:5][CH2:4][CH2:3]1.CN1[C:14](=[O:15])N(C)CCC1.C1C2NC=C(O[C@@H]3O[C@H](CO)[C@H](O)[C@H](O)[C@H]3O)C=2C(Cl)=C(Br)C=1>CO>[CH3:1][N:2]1[C:6](=[O:7])[CH2:5][CH2:4][CH2:3]1.[CH3:14][OH:15]

참가 물질

5

반응물 3

HCID 13387N-methyl-2-pyrrolidone2회HCID 65181X-GalHCID 816462(1H)-Pyrimidinone, tetrahydro-1,3-dimethyl-2회

생성물 1

HCID 22395687NMP Methanol

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Add 7 ml of either NMP or DMPU to 1 gram of X-gal and stir until dissolved. Bring to 10 ml with NMP or DMPU (whichever is already used). Add 90 ml of methanol and mix thoroughly.

후처리

  1. dissolutionuntil dissolved
  2. additionmix thoroughly

출처 및 근거

ORD 기록
ord-fa8b2da9e62f41dda81297dcad4f1235
출처 데이터셋
uspto-grants-2013_08
특허 번호
US08501433B2

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