Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl 4-bromocinnamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | p-Bromocinnamic acid | HCID 99777 | — |
| 생성물 | Methyl 4-bromocinnamate | HCID 816774 | — |
반응 단계
To a stirred solution of 4-bromocinnamic acid (16 g) in methanol (150 mL) was added thionyl chloride (30 mL) at 0° C. The reaction mixture was warmed to room temperature and refluxed for 3 hours. After cooling to room temperature the solvents were evaporated to dryness. The crude compound obtained was used as such for the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08507670B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-1453db34cac84fa79f365c1ae16913b0 |
| 출처 메모 | uspto-grants-2013_08 |