11-Aminoundecanoic acid → N,N,N-Trimethylmethanaminium 11-aminoundecanoate

HRID 1893120노트

반응식

HRID 1893120 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13].[OH-].[CH3:16][N+:17]([CH3:20])([CH3:19])[CH3:18]>O1CCCC1>[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O-:14])=[O:13].[CH3:16][N+:17]([CH3:20])([CH3:19])[CH3:18]

참가 물질

4

반응물 2

HCID 1708311-Aminoundecanoic acidHCID 60966Tetramethylammonium hydroxide

생성물 1

HCID 16212873N,N,N-Trimethylmethanaminium 11-aminoundecanoate

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

Tetramethylammonium 11-aminoundecanoate was synthesized by titration of a methanolic suspension of 11-aminoundecanoic acid (4.04 grams (g) in approximately 4 ml methanol, Aldrich) with methanolic tetramethylammonium hydroxide (8.4 ml, Aldrich), evaporation of the solvent under reduced pressure, and recrystallization from tetrahydrofuran (about 50 ml, Aldrich).

출처 및 근거

ORD 기록
ord-18781f1e58f548db8c82f63860fdca8d
출처 데이터셋
uspto-grants-2013_08
특허 번호
US08512946B2

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