2-Fluorophenol → 2-Fluorophenyl sulfamate

HRID 1893621노트

반응식

HRID 1893621 반응식
C1([O:4][S:5](=[O:8])(=[O:7])[NH2:6])CC1.[F:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[OH:16]>>[F:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[NH:6][S:5](=[O:8])(=[O:7])[O-:4].[F:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[O:16][S:5](=[O:7])(=[O:4])[NH2:6]

참가 물질

4

반응물 2

HCID 97072-FluorophenolHCID 57785190Cyclopropyl sulfamate

생성물 2

HCID 539088522-Fluorophenyl sulfamateHCID 866327902-Fluorophenylsulfamate

실험 절차

2-Fluorophenylsulfamate was synthesized according to the method presented in the synthesis of Sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2-fluorophenol to obtain sulfamic acid 2-fluoro-phenyl ester.

출처 및 근거

ORD 기록
ord-374c0ee81f054b268b0baf980e8c7e81
출처 데이터셋
uspto-grants-2013_08
특허 번호
US08513186B2

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