Benzenesulfonyl chloride → HCID 23372928, 화합물

HRID 1899698노트

반응식

HRID 1899698 반응식
[NH2:1][C:2]1[O:6][N:5]=[C:4]([CH:7]2[CH2:9][CH2:8]2)[C:3]=1[CH3:10].[C:11]1([S:17](Cl)(=[O:19])=[O:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[CH:7]1([C:4]2[C:3]([CH3:10])=[C:2]([NH:1][S:17]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)(=[O:19])=[O:18])[O:6][N:5]=2)[CH2:9][CH2:8]1

참가 물질

3

반응물 2

HCID 7369Benzenesulfonyl chlorideHCID 233729145-Amino-3-cyclopropyl-4-methylisoxazole

생성물 1

HCID 23372928HCID 23372928, 화합물수율 62%

실험 절차

This compound was prepared as described in Example 42 from 5-amino-3-cyclopropyl-4-methylisoxazole and benzenesulfonyl chloride in 62% yield. The crude product was preparative HPLC to give a viscous colorless oil.

후처리

  1. customThis compound was prepared
  2. customto give a viscous colorless oil

출처 및 근거

ORD 기록
ord-cd6af02e14aa4488815060b996eb772c
출처 데이터셋
uspto-grants-1996_11
특허 번호
US05571821

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