Dicyclohexylcarbodiimide → Benzenecarbothioic acid, 4-pentyl-, S-(4-cyanophenyl) ester

HRID 1901402노트

반응식

HRID 1901402 반응식
[CH2:1]([C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=O)=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[C:15]([C:17]1[CH:22]=[CH:21][C:20]([SH:23])=[CH:19][CH:18]=1)#[N:16].C1(N=C=NC2CCCCC2)CCCCC1>CN(C)C1C=CN=CC=1>[CH2:1]([C:6]1[CH:7]=[CH:8][C:9]([C:10]([S:23][C:20]2[CH:21]=[CH:22][C:17]([C:15]#[N:16])=[CH:18][CH:19]=2)=[O:12])=[CH:13][CH:14]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

참가 물질

5

반응물 3

HCID 10868DicyclohexylcarbodiimideHCID 334794-Pentylbenzoic acidHCID 5850584-Thiobenzonitrile

생성물 1

HCID 116614Benzenecarbothioic acid, 4-pentyl-, S-(4-cyanophenyl) ester

시약·촉매·용매 1

HCID 142844-(Dimethylamino)pyridine촉매

실험 절차

Quantities: compound 17 (0.51 g, 3.8 mmol), compound 10 (0.87 g, 4.5 mmol), 4-(dimethylamino)pyridine (0.19 g, 1.6 mmol). N,N'-dicyclohexylcarbodiimide (0.94 g, 4.6 mmol).

출처 및 근거

ORD 기록
ord-e05a528919834e7ea239e330cb4982bd
출처 데이터셋
uspto-grants-1996_11
특허 번호
US05578242

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