Methylhydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

HRID 1902139노트

반응식

HRID 1902139 반응식
Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[CH3:17][NH:18][NH2:19]>CO>[CH3:17][NH:18][NH:19][C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3]

참가 물질

4

반응물 2

HCID 6061MethylhydrazineHCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

생성물 1

HCID 544690901-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The title compound is prepared by reacting the compound of Example 27 (1 mole) with methylhydrazine (1.1 mole) in methanol.

출처 및 근거

ORD 기록
ord-b50d9ee2a7eb4b859e89f04fdbfd22bb
출처 데이터셋
uspto-grants-1996_11
특허 번호
US05578731

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