Epichlorohydrin → HCID 20467884, 화합물
반응식
[OH:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH2:4][CH2:5][C:6]2=O.C1(O)C2C=C[CH:17]=[C:16]([OH:21])[C:15]=2CC1.C(OC1C=CC=C2C=1CCC2O)(=O)C.C(C1OC1)Cl.[OH-].[Na+]>>[O:21]1[CH2:17][CH:16]1[CH2:15][O:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][CH2:6]2참가 물질
6
실험 절차
4-Hydroxy-1-indene is prepared starting from 4-hydroxyindanone via 1,4-indanediol, 4-acetoxy-1-indanol and 4-acetoxy-1-indene in this order. The resulting 4-hydroxy-1-indene is allowed to react with epichlorohydrin in an aqueous solution of sodium hydroxide to give 4-(2,3-epoxypropoxy)indene. [cf. Yakugaku Zasshi 92, 1358 (1972)].
출처 및 근거
- ORD 기록
- ord-98de39b3a9b34b7d876ff60f4a9d45c6
- 출처 데이터셋
- uspto-grants-1984_03
- 특허 번호
- US04435397
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