3-(3-Phenyl-1-propenyl)aniline → 3-(3-Phenylpropyl)aniline
반응식
[C:1]1([CH2:7][CH:8]=[CH:9][C:10]2[CH:11]=[C:12]([CH:14]=[CH:15][CH:16]=2)[NH2:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C(O)C.[C].[Pd]>[C:1]1([CH2:7][CH2:8][CH2:9][C:10]2[CH:11]=[C:12]([CH:14]=[CH:15][CH:16]=2)[NH2:13])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1참가 물질
4
실험 절차
A solution of 3-(3-phenyl-1-propenyl)aniline (3.6 g) in 50 ml of ethanol was subjected to catalytic reduction using 1 g of 10% palladium-carbon. After removal of the catalyst by filtration, the solvent was removed under reduced pressure. The residue was distilled under reduced pressure to give 3.3 g of 3-(3-phenylpropyl)aniline (yield, 92%). B.P. 122°-126° C./0.08 mmHg.
후처리
- customAfter removal of the catalyst
- filtrationby filtration
- customthe solvent was removed under reduced pressure
- distillationThe residue was distilled under reduced pressure
출처 및 근거
- ORD 기록
- ord-14973120f72e4eb5953e84b360c0baf4
- 출처 데이터셋
- uspto-grants-1984_03
- 특허 번호
- US04437880
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