Benzoyl Peroxide → HCID 23438954, 화합물

HRID 1903711노트

반응식

HRID 1903711 반응식
[CH3:1][C:2]1[S:3][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[CH:5][CH:6]=1.[Br:13]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[Br:13][CH2:1][C:2]1[S:3][C:4]([C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=2)=[CH:5][CH:6]=1

참가 물질

5

반응물 3

HCID 7187Benzoyl PeroxideHCID 67184N-bromobutanimideHCID 75788052-methyl-5-phenylthiophene

생성물 1

HCID 23438954HCID 23438954, 화합물

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매

실험 절차

To a boiling solution of 2-methyl-5-phenylthiophene (2g) in dry CCl4 (100 ml) was rapidly added N-bromosuccinimide (1.94 g) and dibenzoylperoxide (0.15 g). After heating under reflux for 30 min., the mixture was cooled and filtered. Evaporation in vacuo gave the title compound as an oil (1.5 g).

후처리

  1. temperatureAfter heating
  2. temperatureunder reflux for 30 min.
  3. temperaturethe mixture was cooled
  4. filtrationfiltered
  5. customEvaporation in vacuo

출처 및 근거

ORD 기록
ord-0902d85f48444f24ad68a2af63c4a5d5
출처 데이터셋
uspto-grants-1984_03
특허 번호
US04438111

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