N-[(Diethoxyphosphoryl)methyl]glycine → Glyphosate

HRID 1903898노트

반응식

HRID 1903898 반응식
C([O:3][P:4]([CH2:9][NH:10][CH2:11][C:12]([OH:14])=[O:13])([O:6]CC)=[O:5])C>Cl>[CH2:11]([NH:10][CH2:9][P:4]([OH:6])([OH:5])=[O:3])[C:12]([OH:14])=[O:13]

참가 물질

3

반응물 1

HCID 12633685N-[(Diethoxyphosphoryl)methyl]glycine

생성물 1

HCID 3496Glyphosate

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

Diethylphosphonomethyl glycine (6 g) was refluxed, for 16 hours, with concentrated hydrochloric acid (20 ml). The reaction mixture was cooled and the solvent was evaporated to obtain glyphosate, which was confirmed by high pressure liquid chromatograph and 31P-nuclear magnetic resonance and infrared spectra.

후처리

  1. temperatureThe reaction mixture was cooled
  2. customthe solvent was evaporated

출처 및 근거

ORD 기록
ord-e3018e0491f94b339c46f88ee9e2d574
출처 데이터셋
uspto-grants-1984_03
특허 번호
US04439373

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