Hydrogen Bromide → HCID 20213264, 화합물

HRID 1905865노트

반응식

[CH2:1]([N:3](C)[CH2:4][CH2:5][CH2:6]O)[CH3:2].[CH2:9]([NH:11][C:12]([NH:14][CH3:15])=[S:13])[CH3:10].Br>>[CH2:9]([NH:11][C:12](=[N:14][CH3:15])[S:13][CH2:6][CH2:5][CH2:4][NH:3][CH2:1][CH3:2])[CH3:10]

참가 물질

반응물 3

HCID 260Hydrogen Bromide

HCID 144409693-[Ethyl(methyl)amino]propan-1-ol

HCID 15568242N-Ethyl-N'-methylthiourea

생성물 1

HCID 20213264HCID 20213264, 화합물

실험 절차

A mixture of 3-(ethylmethylamino)propanol, N-ethyl-N'-methylthiourea and aqueous hydrobromic acid is boiled under reflux to give the dihydrobromide salt of the title compound.

후처리

temperatureunder reflux

출처 및 근거

ORD 기록: ord-d3d35a1a96ba475991b57b0eba5df0c0
출처 데이터셋: uspto-grants-1987_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04649138

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