Sodium Hydroxide → HCID 13713019, 화합물

HRID 1914807노트

반응식

HRID 1914807 반응식
[CH3:1][NH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH2:9].[CH3:10][NH:11][C:12]1[CH:20]=[CH:19][C:15]([C:16](O)=O)=[CH:14][CH:13]=1.[OH-].[Na+]>O>[CH3:10][NH:11][C:12]1[CH:20]=[CH:19][C:15]([C:16]2[N:2]([CH3:1])[C:3]3[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=3[N:9]=2)=[CH:14][CH:13]=1

참가 물질

5

반응물 3

HCID 14798Sodium HydroxideHCID 663454-(Methylamino)benzoic acidHCID 78498N-Methyl-o-phenylenediamine

생성물 1

HCID 13713019HCID 13713019, 화합물

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
80 °C

실험 절차

10.14 mL (86.5 mmol) N-Methyl-o-phenylenediamine and 13.08 g (86.5 mmol) 4-(methylamino)benzoic acid are stirred in 70.0 g polyphosphoric acid at 200° C. for 3 hours. The mixture is cooled to 80° C., poured into water and stirred over night at RT. The mixture is alkalinized with sodium hydroxide solution. The precipitate is filtered off and washed with water. The product is dried in vacuo at 50° C.

후처리

  1. filtrationThe precipitate is filtered off
  2. washwashed with water
  3. customThe product is dried in vacuo at 50° C.

출처 및 근거

ORD 기록
ord-d648c7093ffc4159ad96d844d97e66a5
출처 데이터셋
uspto-grants-2013_12
특허 번호
US08614238B2

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