Acrylic Acid → 2-Propenoic acid, lead(2+) salt

HRID 1921905

반응식

HRID 1921905 반응식
[Pb:1]=O.[OH-].[Na+].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[C:5]([O-:9])(=[O:8])[CH:6]=[CH2:7].[Pb+2:1].[C:5]([O-:9])(=[O:8])[CH:6]=[CH2:7]

참가 물질

4

반응물 3

HCID 6581Acrylic AcidHCID 14798Sodium HydroxideHCID 14827Lead monoxide

생성물 1

HCID 103089162-Propenoic acid, lead(2+) salt수율 93%

실험 절차

111.5 gms of lead monoxide is taken in 0.1 NaOH and the mixture stirred in a round bottom flask for 30 minutes at room temperature, 72 gms of acrylic acid is then adding by a dropping funnel and a period of 1 hour. The mixture is heated under reflux conditions to 35° C. for 1 hour. The yield was 93% of lead acrylate after filtration, washing and drying.

후처리

  1. temperatureThe mixture is heated under reflux conditions to 35° C. for 1 hour

출처 및 근거

ORD 기록
ord-2efc357025694a09b2d39f0e11906115
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08173754B2

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