6-Chloroindole → HCID 178419815, 화합물

HRID 1938025노트

반응식

HRID 1938025 반응식
CC1(C)OB(c2ccc3ncn(C4CCOCC4)c3c2)OC1(C)C.Clc1ccc2cc[nH]c2c1>C1CCOC1.CC(C)c1cc(C(C)C)c(-c2ccccc2P(C2CCCCC2)C2CCCCC2)c(C(C)C)c1.Nc1ccccc1-c1[c-]cccc1.O.O=P([O-])([O-])[O-].[Cl][Pd+].[K+].[K+].[K+]>c1cc2ccc(-c3ccc4ncn(C5CCOCC5)c4c3)cc2[nH]1

참가 물질

8

반응물 2

HCID 871116-ChloroindoleHCID 529880091-(Tetrahydro-2H-pyran-4-yl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d]imidazole

생성물 1

HCID 178419815HCID 178419815, 화합물수율 26%

시약·촉매·용매 5

HCID 62657Potassium Phosphate, Tribasic시약HCID 54727932[2-(2-Aminophenyl)phenyl]-chloro-palladium dicyclohexyl-[2-(2,4,6-triisopropylphenyl)phenyl]phosphane촉매HCID 962Water용매HCID 8028Tetrahydrofuran용매2회HCID 741954,4'-Bis(1,1-dimethylethyl)-1,1'-biphenyl내부 표준

반응 조건

온도
25 °C

후처리

  1. stirring기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-c0781594895c46a6829faf8f2876c6db
출처 데이터셋
Pd_CN_Coupling_Informer_Library
원본 링크
출처 보기

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