Triphenylphosphine → HCID 178506034, 화합물
반응식
[F:1][CH2:2][CH2:3][CH2:4][Br:5].[C:6]1([P:12]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>C1(C)C=CC=CC=1>[Br-:5].[F:1][CH2:2][CH2:3][CH2:4][PH:12]([C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1)([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1참가 물질
4
실험 절차
3-Fluorobromopropane (200.0 g, 1.42 mol) was dissolved in toluene (3), followed by adding to the solution, triphenylphosphine (37.2 g, 1.42 mol), refluxing the mixture for 15 hours, filtering off the resulting product, and suction-drying, to obtain 3-fluoropropyltriphenylphosphine bromide (486 g, 1.21 mol). Yield: 85.2%.
후처리
- temperature