Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl(4-nitrophenyl)phosphonate → P-(4-Nitrophenyl)phosphonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl(4-nitrophenyl)phosphonate | HCID 284865 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | P-(4-Nitrophenyl)phosphonic acid | HCID 196997 | 100% |
반응 단계
A solution of diethyl(4-nitrophenyl)phosphonate (60 g, 230 mmol) in 250 mL of concentrated HCl (aq) was stirred at reflux overnight. The excess HCl was removed under reduced pressure and the product used in further chemistries without purification (46.8 g, yield: 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08399433B2 |
| 출처 데이터셋 | uspto-grants-2013_03 |
| ORD ID | ord-3b0357372e794db29131a38f1aeb1aa9 |
| 출처 메모 | uspto-grants-2013_03 |