Triethyl phosphite → Diethyl(4-amino-3-methoxybenzyl)phosphonate

HRID 1947801노트

반응식

HRID 1947801 반응식
C(P(C[CH2:7][C:8]1[CH:13]=[CH:12][C:11]([NH2:14])=[C:10]([O:15][CH3:16])[CH:9]=1)(=O)[O-])C.[CH2:17]([O:19][P:20]([O:24]CC)[O:21][CH2:22][CH3:23])[CH3:18]>>[CH2:17]([O:19][P:20]([CH2:7][C:8]1[CH:13]=[CH:12][C:11]([NH2:14])=[C:10]([O:15][CH3:16])[CH:9]=1)(=[O:24])[O:21][CH2:22][CH3:23])[CH3:18]

참가 물질

3

반응물 2

HCID 31215Triethyl phosphiteHCID 86653998Ethyl(4-amino-3-methoxybenzyl)methylphosphinate

생성물 1

HCID 86653997Diethyl(4-amino-3-methoxybenzyl)phosphonate

실험 절차

This material was prepared according to the procedure described above for ethyl(4-amino-3-methoxybenzyl)methylphosphinate using triethylphosphite in the first step. MS (ES+): m/z 274.01 [MH+] (ZQ3, polar 5 min).

후처리

  1. customThis material was prepared
  2. customm/z 274.01 [MH+] (ZQ3, polar 5 min)

출처 및 근거

ORD 기록
ord-15752ec06e8c444891901f37631ed3e4
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08399433B2

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