HCID 54370181, 화합물 → HCID 10451888, 화합물
반응식
[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([N:8]=[C:9]([O:16]C)[C:10]([O:14]C)=[N:11]2)=[C:6]([CH2:18][N:19]([CH2:28][CH3:29])[C@H:20]([P:22](=[O:27])([O:25]C)[O:23]C)[CH3:21])[CH:5]=1)([O-:3])=[O:2]>Cl>[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:16])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:18][N:19]([CH2:28][CH3:29])[C@H:20]([P:22](=[O:23])([OH:27])[OH:25])[CH3:21])[CH:5]=1)([O-:3])=[O:2]참가 물질
3
실험 절차
4.24 g (9.9 mmol) of dimethyl (R)-N-(7-nitro-2,3-dimethoxyquinoxalin-5-ylmethyl)-α-ethylaminoethylphosphonate are stirred for 19 hours in 80 ml of 6N hydrochloric acid. The reaction mixture is evaporated and the residue is slurried with water. The title compound is obtained as a solid of m.p.=218° C. (dec.).
후처리
- customThe reaction mixture is evaporated
출처 및 근거
- ORD 기록
- ord-6d37ef974b8448ee98e381f1fd502791